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Most manufacturers conducted the monitoring of nonsterile pharmaceutical manufacturing environments. Companies producing topicals, liquids, and aerosols tend to have more extensive programs than those companies manufacturing tablets or other solid oral dosage forms. Among the nonsterile manufacturing environments monitored were air, processing equipment, and water. Air quality was monitored using centrifugal air samplers, settling plates, and so on. Product contact surfaces of equipment were monitored using swabs or contact plates, with swabs being preferred because of better access of irregular surfaces. Since swabs used are presterilized, they are less likely to contaminate the surface being sampled, whereas contact plates which contain nutrient agar media may encourage growth of microorganisms after sampling, unless the sampled area is thoroughly cleaned with ethanol or other sterilizing agent. However, contact plates are easier to use on plain at surfaces and also help provide an accurate assessment of in situ microbial status. Companies with monitoring programs have established alert and action limits. Alert levels of microorganisms may indicate a change from normal operating procedures but may not require any corrective action, whereas action levels may suggest a signi cant change from normal operating procedures and require corrective actions to control further proliferation of microbes. 6.3.5.2 Recommendations

To add a frame to an existing frameset, you drag the single-frame icon from the Frames tab of the Objects palette and release the mouse where you wish the new frame to be placed You can also add another frameset to the frameset on your page by dragging another frameset icon into place Inserting frames or framesets within an existing frameset can be tricky, so here are a few clues to guide you: If you have two vertical frames and want to add a third vertical frame between them, drag the new frame icon onto the line that divides them If you have two horizontal frames and want to add a third horizontal frame between them, drag the new frame icon onto the line that divides them To divide a vertical frame into two, drop the new frame within the page area of the existing frame.

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Regardless of whether you drop the new frame to the top or bottom of the existing frame, the new section appears at the bottom The frame into which the new frame lands becomes outlined by a dark line within the frame To divide a horizontal frame into two, drop the new frame within the page area of the existing frame Regardless of whether you drop the new frame to the left or right side of the existing frame, the new section appears at the right The frame into which the new frame lands becomes outlined by a dark line within the frame Dropping an entire frameset works the same way; you either drop it onto the border between frames or into a frame s area Dropping a frameset onto a border adds the new frames between the existing frames.

Dropping a new set into a frame subdivides that frame s space Remember, you always have the Undo command (Edit Undo); you ll need it while getting the hang of inserting frames..

In the second step, achiral 9-borabicyclo[3.3.1]nonane (9-BBN) adds to the less hindered diastereotopic face of -pinene to yield the chiral reducing agent Alpine-Borane. Aldehydes are rapidly reduced to alcohols. The reaction with deuterio-Alpine-Borane, which yields (R)- -d-benzyl alcohol in 98% enantiomeric excess (ee) reveals a very high degree of selectivity of the enantiotopic faces of the aldehyde group in a crowded transition state:

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charge There should be little di erence in the slopes of lines c and d since the metal center is the same However, the HOMO LUMO gap decreases since NH3 has a weaker trans e ect than Cl (see above) The interactions primarily responsible for the binding of the alkene are shown by bold dashed or dotted lines labeled i, ii, and iii The attractive interaction, i, which is responsible for the majority of the binding energy, clearly is the weakest in Zeise's complex and increases in both series due to the slopes of lines b and d At the same time, in both series, the attractive interaction, iii, decreases due to the slopes of lines a and c.

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